SPECTROSCAN МАКС-GVM

“SPECTROSCAN MAKC-GVM” WDXRF spectrometer determines elements from Na (Sodium) to U (Uranium) in solids, liquids or powders, in solutions and thin films, deposits on filters.
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“SPECTROSCAN MAKC-GVM” WDXRF spectrometer determines elements from Na (Sodium) to U (Uranium) in solids, liquids or powders, in solutions and thin films, deposits on filters.
The spectrometer operation is based on irradiation of the sample with primary X-rays generated by X-ray tube, registration of the secondary fluorescence from the sample elements preliminary diffracted on a crystal, and calculation of the elements concentration with the help of calibration equation, which is a relation between the element concentration and intensity of the registered secondary emission from the element. The spectrometer has high resolution of spectral lines and therefore provides accurate determination of elements in complicated multicomponent substances.

Advantages

Non-destructive analysis – all elements in the range from Na (Sodium) to U (Uranium) can be determined from one sample. Desk top spectrometer doesn’t require water supply or gas supply systems.

The measuring system of the spectrometer in the vacuum chamber while the samples are at the ambient pressure, so no He is required for the sample chamber and all samples (including liquid and powder) may be studied without any special measures taken.

Spectrum scanning and high resolution of crystal analyzers excludes close lines of different elements overlapping (therefore there is no need in their mathematical differentiation), provides correct background accounting. All these provide accuracy and reliability of analysis.

Automatic sample changer for 10 samples with two spinning samples for analysis of non-homogeneous samples minimizes need of operator activity while measurements.

The spectrometer is delivered precalibrated for customer’s analytical tasks, with required accessories set and sample preparation equipment if necessary.

Learn more

“SPECTROSCAN MAKC-GVM” is a desk top WDXRF spectrometer controlled by an internal computer.
There are two blocks in it: spectrometric with closed cycle water cooling system and vacuum pump.

Spectrometric bloc is equipped with X-ray tube power of 160 W with a side output of radiation, goniometer, located in an evacuated volume, four automatically interchangeable analyzer crystal, two-chamber radiation detector, automated multiposition sample changer device.

 Technical specification 
X-ray tube anode voltage
40 kV
X-ray tube capacity
up to 160 W
X-ray tube anode
Pd (or Cr)
Spectral resolution
Crystal diffractio
Four crystal analyzers
LiF(200), C(002), PET, KAP
Sample changer
10 sample automatic
2 spinning samples
Power supply
220 V, 50 Hz
Analytical parameters 
Determined elements from Na to U
Energy resolution 9 eV (Si Kα), 60 eV (Fe Kα)

Technical details

"SPECTROSCAN MAKC-GV" is a desk top WDXRF spectrometer controlled by an external computer.
There are three blocks in it: spectrometer, vacuum pump and closed cycle water cooling system.

The measuring system of the spectrometer is in the vacuum chamber while the samples are at the ambient pressure, so no He is required for the sample chamber and all samples (including liquid and powder) may be studied without any special measures taken.

The Spectrometer is controlled with external computer.

ANALYTICAL PARAMETERS
Determined elements from Na to U
Energy resolution 9 eV (Si Kα), 60 eV (Fe Kα)
TECHNICAL SPECIFICATION
X-ray tube anode voltage 40 kV
X-ray tube capacity up to 160 W
X-ray tube anode Pd (or Cr)
Spectral resolution Crystal diffraction
Four crystal analyzers LiF(200), C(002), PET, KAP
Sample changer 10 sample automatic
2  spinning samples
Power supply 220 V, 50 Hz
Consumed capacity from  220 V mains 850 W
PC interface USB
No additional gas required
Closed cycle water cooling system

Water analysis

X-ray fluorescence analysis (XRFA) is one of the methods applied for element concentration determination of water objects. The material for analysis may vary from potable water to sea water, from snow to wastewaters. The advantage of this method is simplicity of determination of multi elemental composition in one sample, low consumption of auxiliary materials, The following problems may be solved with XRFA: - determination of dissolved and not solved metal forms in water, as well as their total content; - element content in suspensions; - element content in snow. Element content can  be determined either directly or after concentration dependent on the type of sample material. Direct determination of element content by XRFA begins from first mg/L in the range from Mg up to U. In case of direct determination the sample material is filtered from suspension and mechanical impurity, and then poured in a sample cup, placed into spectrometer. Analysis is carried out according to the chosen program automatically. No additional sample preparation is required. Elements of the suspension are determined after concentration on membrane filter. Water sample material is pumped through the membrane filter; the filter is dried, fixed in a filter holder and placed into spectrometer. Sensitivity of analysis is first micrograms per filter, therefore it is possible to determine element content of 1-5 microgram/l after concentration of one liter of water sample material. Heavy metal determination is usually carried out after concentration because of low content of heavy metals in  water objects. There are two types of concentrating procedures offered: Sorption concentrating with cellulose filters. Sample material is pumped through the filter with sedimented aminocarboxylic groups at a preset speed. Heavy metals from the water material are fixed inside the filter. The filter is dried, fixed in a filter holder and placed into a spectrometer. When total element forms are determined, nitric acid is added to the sample, and then it is evaporated to wet salts state, which are solved further on in distilled water and pumped through the filter. This type of concentrating is usually used for potable water, because the filter has limited sorption capability. Sedimentation of  metal organic complex on filter. The sample material is mixed with ammonium pirrolidinditiocarbaminate in dynamic regime. Obtained insoluble complexes are precipitated on paraffin filter. After concentrating on filter the sample filter is dried, fixed in a filter holder and placed into spectrometer. When total element forms are determined, nitric acid is added to the sample, and then it is evaporated to wet salts state, which are solved further on in distilled water and pumped through the filter.